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This textbook has been specifically developed as per latest curriculum on the directives of NEP 2020 - For the Universities of Uttar Pradesh for B. Sc. Students of Chemistry for the Fifth Semester. Maintaining the traditional approach to the subject, Theory part comprehensively covers important topics such as Alkanes, Cycloalkanes, Chemistry of Alkenes, Alkynes, Aromaticity & Arenes, Alcohols, Phenols, Ethers & Epoxides, and Chemistry of Organic Halides. All chapters have been presented systematically to help students in Achieving Solid Conceptional understanding and learn experimental procedures. Practical Part covers Elemental analysis and Identification of functional groups, Separation of Organic Mixture and identification of organic compounds presented systematically to help students in achieving solid conceptional understanding and learn experimental procedures.